Research
▼ Contents
・ How to design non-equilibrium materials created by metal additive manufacturing?
・ How to design materials using impurity elements believed to be harmful?
・ How to design hot-dip galvanizing coatings for steel surfaces?
・ Fundamentals of crystal plasticity in designed materials
・ How to design non-equilibrium materials created by metal additive manufacturing?
・ How to design materials using impurity elements believed to be harmful?
・ How to design hot-dip galvanizing coatings for steel surfaces?
・ Fundamentals of crystal plasticity in designed materials
Understanding Micro/Nanostructures, Innovating Materials
Our team explores the fundamentals of controlling micro- and nano-structures produced by various manufacturing processes for structural metallic materials. Based on the fundamentals, we design elemental compositions and production processes to create innovative structural materials with high and multi-functionality. We will also use micromechanical testing and in-situ observation to explore the nature of plastic deformation of metal crystals to improve further mechanical performance.
We would like to encourage students and young researchers to hone their abilities and develop their skills through independent research activities. We have an international membership, including international students and researchers, and actively collaborate with other universities, research institutes, and industries to keep high activity in each research.
How to design non-equilibrium materials created by metal additive manufacturing?
Metal additive manufacturing (often denoted as “Metal 3D Printers”) can control not only “topology" but also "property”.Laser powder bed fusion (L-PBF) with metal powders, a type of additive manufacturing known as metal additive manufacturing, can produce components with complex three-dimensional shapes that are impossible with conventional manufacturing processes. The metal components produced by the L-PBF process are manufactured via an ultrafast solidification process (a phenomenon in which liquid metal transforms to solid at a high cooling speed above 1 million degrees per second) by scanning laser irradiation.
Our team focuses on the micro- and nano-structure produced by the L-PBF process, which is characterized not only by being very refined but also by being in a non-equilibrium state. Such a non-equilibrium state created by the L-PBF process not only dramatically improves the performance of metallic materials but also creates anomalous physical properties that are sometimes opposite to the common sense of materials science. Material design using nonequilibrium states created by metal additive manufacturing technologies can be applied not only to Al alloys, but also to various metals, and we are developing copper alloys, steels, and composite materials. Based on the fundamental understanding, we will use computational calculations to optimize chemical compositions in multi-elemental systems and produce materials with innovative high functionality and multifunctionality using metal additive manufacturing technologies.
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Related papers
- N. Takata, M. Liu, H. Kodaira, A. Suzuki, M. Kobashi, Anomalous strengthening by supersaturated solid solutions of selectively laser melted Al–Si-based alloys, Additive Manufacturing, vol. 33, 101152, (2020).
- N. Takata, M. Liu, H. Li, A. Suzuki, M. Kobashi, Fast scanning calorimetry study of Al alloy powder for understanding microstructural development in laser powder bed fusion, Materials & Design, vol. 219, 110830, (2022).
- N. Takata, M. Liu, A. Suzuki, M. Kobashi, M. Kato, Negative strain rate sensitivity of yield strength of Al-Si alloy additive-manufactured using laser powder bed fusion, Scripta Materialia, vol. 213, 114635, (2022)
- D. Kim, N. Takata, J. Umeda, T. Shimizu, M. Kobashi, Anomalous temperature-dependent strength of copper alloy manufactured by laser-beam powder bed fusion, Additive Manufacturing Letters, Vol. 11, 100236, (2024).
How to design materials using impurity elements believed to be harmful?
Aluminum (Al) is produced from a raw material called "bauxite" through an electrolytic refining process, and all new Al ingots are imported from overseas due to the amount of electricity used in the domestic electrolytic refining process. On the other hand, the use of recycled Al can reduce CO2 emissions during production by 97% compared to the use of new ingots, making efforts to promote a recycling-oriented economy an urgent necessity from a carbon-neutral perspective. A large amount of scrap aluminum alloys, which are commonplace in our daily lives, contain many impurities, such as silicon (Si) and iron (Fe). These elements are usually removed because they form intermetallic compounds with Al, making the materials brittle and degrading.Our team aims to effectively utilize impurity elements (Fe, Si, Mn, etc.) that are considered harmful and to achieve high mechanical performance for Al alloys by using casting and heat treatments, which are the production processes of Al alloys. We will establish principles for controlling micro- and nanostructures using impurity elements by using theoretical calculations and electron microscope analysis techniques and design Al alloy component utilization and processes to realize improved recycling.

Related papers
- N. Okano, N. Takata, A. Suzuki, M. Kobashi, Effects of Mn and Cu Additions on Solidification Microstructure and High-Temperature Strength of Cast Al–Fe Binary Alloy, Materials Transactions, vol. 64 (2), 492-499, (2023).
- W. Wang, N. Takata, A. Suzuki, M. Kobashi, M. Kato, Design of Al–Fe–Mn alloy for both high-temperature strength and sufficient processability of laser powder bed fusion, Additive Manufacturing, vol. 68, 103524, (2023).
How to design hot-dip galvanizing coatings for steel surfaces?
As described in high school chemistry textbooks, hot-dip zinc (Zn) galvanizing surface treatment (coating) technology provides high corrosion resistance (sacrificial corrosion protection), which is an important environmental resistance property for steels. Hot-dip Zn galvanizing is applied to various structural steels and is one of the leading products in the Japanese steel industry. Therefore, the technology of the hot-dip galvanizing process (development technology of high-performance surface-treated steels) is directly related to corporate profits in the steel industry, and the research results within companies are accumulated as know-how, most of which are not open to the public, and the fundamental knowledge that can be shared is limited so far.Our team, belonging to a university as a neutral position, conducts fundamental studies for the development of high-functional and multifunctional hot-dip galvanized coatings that are not limited to environmental resistance and builds an academic foundation for innovation in hot-dip galvanizing technology. Based on theoretical calculations, we not only understand the formation mechanism of micro- and nanostructures through the solid-liquid reaction process in the hot-dip galvanizing process but also elucidate the dominant factors contributing to mechanical functions such as workability using experimental methods combined with electron microscopy techniques.
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Related papers
- D. Kim, N. Takata, H. Yokoi, A. Suzuki, M. Kobashi, Microstructural factors controlling crack resistance of Zn–Al–Mg alloy coatings prepared via hot-dip galvanizing process: Combined approach of in-situ SEM observation with digital image correlation analysis, Journal of Materials Research and Technology, vol. 29, 1535-1541, (2024).
- H. Yokoi, N. Takata, A. Suzuki, M. Kobashi, Formation sequence of Fe–Al intermetallic phases at interface between solid Fe and liquid Zn–6Al–3Mg alloy, Intermetallics, vol. 109, 74-84, (2019).
- N. Takata, M. Nishimoto, S. Kobayashi, M. Takeyama, Crystallography of Fe2Al5 phase at the interface between solid Fe and liquid Al, Intermetallics, vol. 67, 1-11, (2015).
Fundamentals of crystal plasticity in designed materials
A micropillar compression test is a method of investigating mechanical properties by fabricating micropillars of a few micrometers in size from a specific region in the small samples using a Focused Ion Beam (FIB) system and performing compression tests using a nanoindenter system. This technique is useful for fundamental studies on the strength and deformation of various materials because it is easy to perform compression tests on single-crystals.In our team, we take advantage of the ability to experimentally measure the mechanical properties of specimens made from a specific region of a microscopic specimen under electron microscopy to investigate the mechanical properties of not only metal/alloys but also the constituent phases within composite or multi-phase materials in terms of crystal plasticity. In addition, since the test can be performed in a limited volume, experimental measurements of the strength and plastic deformation of surface coating materials and powder particle materials developed at various universities and research institutes in Japan and overseas are also performed. The micropillar compression test can provide insight into the deformation mechanism of novel materials.

Related papers
- T. Zhu, N. Takata, D. Kim, M. Kobashi, M. Yoshino, M. Tsukamura, Effect of Cr content on thermally activated deformation in single-crystal micropillars of Fe–Cr binary alloys, Materials Science and Engineering: A, vol. 900, 146499, (2024).
- H. Li, T. Zhu, N. Takata, M. Kobashi, M. Yoshino, Thermal activation process of plastic deformation in Fe–18Cr single-crystal micropillars with high-density dislocations, Materials Science and Engineering: A, vol. 819, 141459, (2021).
- N. Takata, S. Takeyasu, H. Li, A. Suzuki, M. Kobashi, Anomalous size-dependent strength in micropillar compression deformation of commercial-purity aluminum single-crystals, Materials Science and Engineering: A, vol. 772, 138710, (2020).
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